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![loading](/sites/all/modules/hf_eds/images/loading.gif)
A Knoevenagel Initiated Annulation Reaction Using Room Temperature or Microwave Conditions
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![loading](/sites/all/modules/hf_eds/images/loading.gif)
- Author(s): Cook, A. Gilbert
- Language:
English- Source:
Journal of Chemical Education. Sep 2007 84(9):1477-1479.- Physical Description:
PDF- Publication Date:
2007- Document Type:
Journal Articles
Reports - Evaluative- Online Access:
- Language:
- Additional Information
- Availability: Division of Chemical Education of the American Chemical Society. Subscription Department, P.O. Box 1267, Bellmawr, NJ 08099-1267. Tel: 800-691-9846; Tel: 856-931-5825; Fax: 856-931-4115; e-mail: [email protected]; Web site: http://www.jce.divched.org
- Peer Reviewed: Y
- Source: 3
- Education Level: Higher Education
- Subject Terms:
- ISSN: 0021-9584
- Abstract: An experiment is presented that has the student execute a Knoevenagel initiated annulation reaction. The reaction can be carried out either through use of a microwave reactor or by allowing the mixture to stand at room temperature for two days. The student is then challenged to identify the reaction product through a guided prelab exercise of the synthesis of the Hagemann ester, and then through GC-MS, NMR, and IR spectra of the product. The stereochemistry of the product is determined through the NMR spectrum and the Karplus curve. The student is required to write a mechanism for the reaction. (Contains 2 figures.)
- Abstract: As Provided
- Number of References: 20
- Publication Date: 2008
- Accession Number: EJ820775
- Availability:
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