Design of encapsulation method for chlorogenic acid and caffeine in coffee waste by-product.

Publisher: Wiley Country of Publication: England NLM ID: 9200492 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1099-1565 (Electronic) Linking ISSN: 09580344 NLM ISO Abbreviation: Phytochem Anal Subsets: MEDLINE

Original Publication: Chichester, Sussex, UK : Wiley, c1990-

Chlorogenic Acid*/analysis ; Chlorogenic Acid*/chemistry ; Caffeine*/analysis ; Caffeine*/chemistry ; Coffee*/chemistry; Waste Products/analysis ; Powders/chemistry ; Seeds/chemistry ; Solubility ; Spray Drying

Introduction: Coffee silver skin (CSS) is a thin covering over green coffee seeds inside coffee cherry. It is a good source of bioactive compounds like chlorogenic acid and caffeine. It is produced as a by-product of the roasting process.
Objective: The goal of this study is to apply spray drying method to encapsulate 5-O-caffeoylquinic acid (chlorogenic acid) and caffeine extracted from CSS.
Methods: The main-plots for optimisation were feed solid concentration (2.5, 5, 10°Bx), and the sub-plots of the whole-plot were carrier material type (maltodextrin, modified starch, arabic gum) and inlet air temperature (130, 160, 190°C). Responses included were drying yield, chlorogenic acid concentration, caffeine content, Carr index, and solubility values.
Results: Suitable conditions were spray drying inlet temperature of 190°C, extract concentration of 10°Bx, and wall material composition [modified starch/arabic gum (MS:AG)] 10.5:9.5. As the feeding CSS extract concentration increased, the amount of chlorogenic acid and caffeine in the final powder increased, while the powder's flow characteristics improved.
Conclusions: The concentration stage might be used to produce free-flowing powdered particles with good bioactive retention for use in the food processing industry.
(© 2023 John Wiley & Sons Ltd.)

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Keywords: bioactive compounds; caffeine; coffee silver skin powder; encapsulation; spray drying

318ADP12RI (Chlorogenic Acid)
3G6A5W338E (Caffeine)
0 (Coffee)
0 (Waste Products)
0 (Powders)

Date Created: 20230125 Date Completed: 20241203 Latest Revision: 20241203

20241204

10.1002/pca.3207

36694947