The effect of hydrofluoric acid concentration on the fatigue failure load of adhesively cemented feldspathic ceramic discs.

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  • Additional Information
    • Source:
      Publisher: Elsevier Science Country of Publication: England NLM ID: 8508040 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1879-0097 (Electronic) Linking ISSN: 01095641 NLM ISO Abbreviation: Dent Mater
    • Publication Information:
      Publication: 1998- : Kidlington, Oxford, UK : Elsevier Science
      Original Publication: Copenhagen : Munksgaard, c1985-
    • Subject Terms:
      Acid Etching, Dental* ; Dental Restoration Failure*; Aluminum Silicates/*chemistry ; Dental Cements/*chemistry ; Hydrofluoric Acid/*chemistry ; Potassium Compounds/*chemistry ; Resin Cements/*chemistry; Ceramics/chemistry ; Dental Stress Analysis ; In Vitro Techniques ; Materials Testing ; Surface Properties
    • Abstract:
      Objective: This study investigated the influence of hydrofluoric acid (HF) etching at different concentrations on the fatigue failure load of adhesively cemented feldspathic ceramic discs (Vita Mark II). Besides, their effect on the micromorphology of ceramic surface was investigated.
      Methods: Eighty ceramic discs (ϕ=10 mm; thickness=1.5 mm) were cemented to epoxy supporting discs (ϕ=10 mm; thickness=2.0mm) using different surface conditioning methods (n=20): nonetched control (CTRL), or etched for 60s with different HF concentrations: 1% (HF1), 5% (HF5), or 10% (HF10). All the ceramic discs received a silane application (Monobond Plus). The epoxy discs were etched with 10% HF for 60s and received a primer coating (Multilink Primer A+B). Adhesively cementation was performed (Multilink Automix), and the assemblies (ceramic discs/epoxy discs) were subjected to cyclic loads in water by a staircase approach (500,000 cycles; 20Hz; initial load=290N; step size=30N). Fatigue failure load data were analyzed using 1-way ANOVA and post-hoc Tukey's tests (α=.05).
      Results: Mean failure load of the HF5 group (255.0±23.0N) was significantly lower; HF1 group (301.7±71.0N) presented intermediate values, and the highest values were achieved in CTRL (351.7±13.4N) and HF10 (341.7±20.6N) groups. All the failures were radial cracks starting from the bonding surface.
      Significance: In terms of fatigue failure load, etching with 1% and 5% HF had a deleterious effect on the fatigue behavior of an adhesively cemented feldspathic ceramic, while 10% HF had no negative influence.
      (Copyright © 2018 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.)
    • Contributed Indexing:
      Keywords: Acid etching; Fatigue; Glass ceramics; Mechanical cycling; Surface treatment
    • Accession Number:
      0 (Aluminum Silicates)
      0 (Dental Cements)
      0 (Monobond S)
      0 (Potassium Compounds)
      0 (Resin Cements)
      0 (multilink adhesive system)
      12168-80-8 (feldspar)
      RGL5YE86CZ (Hydrofluoric Acid)
    • Publication Date:
      Date Created: 20180205 Date Completed: 20190123 Latest Revision: 20220331
    • Publication Date:
      20221213
    • Accession Number:
      10.1016/j.dental.2018.01.010
    • Accession Number:
      29397196