Trace analysis of volatile N-nitroso compounds by combined gas chromatography and thermal energy analysis.

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  • Author(s): Fine DH; Rounbehler DP
  • Source:
    Journal of chromatography [J Chromatogr] 1975 Jun 18; Vol. 109 (2), pp. 271-9.
  • Publication Type:
    Journal Article
  • Language:
    English
  • Additional Information
    • Source:
      Publisher: Elsevier Country of Publication: Netherlands NLM ID: 0427043 Publication Model: Print Cited Medium: Print NLM ISO Abbreviation: J Chromatogr Subsets: MEDLINE
    • Publication Information:
      Original Publication: Amsterdam, Elsevier.
    • Subject Terms:
      Chromatography, Gas/*methods ; Nitroso Compounds/*analysis; Cold Temperature ; Diethylnitrosamine/analysis ; Dimethylnitrosamine/analysis ; Methylene Chloride/analysis ; Nitrosamines/analysis ; Piperidines/analysis ; Pyrrolidines/analysis ; Sarcosine/analogs & derivatives
    • Abstract:
      Thermal energy analysis (TEA) has been combined with gas chromatography (GC). The new GC-TEA technique is highly specific to compounds which contain heat labile nitrosyl groups. Because of the specificity of the technique, full use may be made of the TEA sensitivity. Analysis by direct injection of solutions containing less than 1 ng/ml N-nitroso compound is demonstrated.
    • Accession Number:
      0 (Nitrosamines)
      0 (Nitroso Compounds)
      0 (Piperidines)
      0 (Pyrrolidines)
      3IQ78TTX1A (Diethylnitrosamine)
      588X2YUY0A (Methylene Chloride)
      M43H21IO8R (Dimethylnitrosamine)
      Z711V88R5F (Sarcosine)
    • Publication Date:
      Date Created: 19750618 Date Completed: 19751105 Latest Revision: 20190629
    • Publication Date:
      20221208
    • Accession Number:
      10.1016/s0021-9673(01)91799-6
    • Accession Number:
      1150821